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The following PDF documents should help you with many aspects of your CapNMR and OneMinuteNMR system. MaintenanceProbe and system maintenance recommendations. | Shipping Instructions | PDF, 225k
| How to ship your probe back, if that ever becomes necessary.
| | One Minute NMR Moving Instructions | PDF, 59k
| How to shutdown, disconnect, physically move, and repower the OMNMR Discovery Tower and Leap autosampler | Probe blockage trouble shooting and maintenance. | PDF, 212k | How to prevent, trouble shoot, and remove flow blockages.
| One Minute NMR Consumables
| PDF, 68k
| A list of items you will need to replenish occasionally.
| Pulse Width Calibration Sample (TXI probe only) | PDF, 7kB
| The recipe for the standard sample used for calibrating N15 and C13 indirect pulsewidths. |  [NEW] Cleaning Procedure with Oxalic Acid added 2009-09-04 | PDF, 14kB
| Oxalic acid is a very effective method of cleaning your probe. This document gives details on how to go about giving your probe a good cleaning. |
NMRThe following technical bulletins will help you take data with your CapNMR probe. For further information, you may want to look at the available sample data sets. (TODO: insert link here) | Proton for CapNMR | PDF, 97k
| How to take H1 data.
| | CapNMR shimming tutorial. | PDF, 240k
| The CapNMR probe is easy to shim, but it shims much differently than a tube probe.
| Indirect C13 Pulsewidth Calib. (Varian) Indirect C13 Pulsewidth Calib. (Bruker) | PDF, 24k | How to calibrate the C13 indirect pulsewidth on your CapNMR probe.
| Direct Carbon for CapNMR (C20) or Direct Carbon for CapNMR (L30) | PDF, 100k, 150k
| How to take direct C13 data.
| Background subtraction for direct Carbon.
| PDF, 158k
| The CapNMR probe has a small background signal when used for direct C13. Here's how to get rid of it.
| gCOSY for CapNMR
| PDF, 95k
| COSY
| TOCSY
| PDF, 93k
| TOCSY
| NOESY
| PDF, 95k
| NOESY
| NOESY1D
| PDF, 130k
| NOESY1D | gHSQC
| PDF, 97k
| gHSQC
| gHMBC
| PDF, 94k
| gHMBC
| | CapNMR probe positioning and calibration for Bruker spectrometers | PDF, 566k
| How to position your CapNMR probe and calibrate it in a Bruker spectrometer.
| | MicroFlow NMR Reference Model Compounds | PDF, 12k
| Recipes for practical model and reference compounds, useful for testing a One Minute NMR Installation. |
Sample Preparation, Containers and Filtration
Fluidics | Mini Manual Injection Kit and Description - Customers | PDF, 75k
| How to assemble the MMIK, including component vendors and part numbers | | Mini Manual Injection Optimization of Solvent Push Volume | PDF, 4k
| A diagram of simulated S/N vs push volume calibration | HTSL FEP Plumbing Tutorial
| PDF, 2.5M
| How to interface your HTSL pump with FEP tubing.
| Fluidic Connections
| PDF, 1.1M
| How to form fluidic connections between pieces of tubing, and between tubing and different objects. | Fused silica capillary tutorial
| PDF, 985k | How to work with the old style tubing.
| | MIM conversion | PDF, 1.7M
| How to convert your MIM from fused silica to FEP.
| Connecting FEP to CapNMR probe
| PDF, 169k
| How to connect FEP tubing to the CapNMR probe.
| Syringe Vise and Clamp
| PDF, 48k
| How to use the syringe vise and clamp for manual injections. | | FEP tubing tutorial | PDF, 1017k
| How to use FEP tubing for a variety of purposes.
| Valco Inline Filter
| PDF, 296k
| How to install and change the Valco inline filter (CUCKF) used for both automation and manual injection. | | One Minute NMR Leap Autosampler Tray Changes | PDF, 11k
| How to change the tray on the Leap Autosampler through One Minute NMR | | LEAP PAL valve maintenance | PDF, 922k
| How to maintain the LC valve on your LEAP/CTC PAL. | Installation Notes
OMNMR Computer prereqs
| PDF, 306k
| Things you or your IT people need to have set up prior to an installation of OMNMR.
| Installation Checklist
| PDF, 145kB | This document contains a checklist of tasks that must be completed by the customer prior to an installation of One Minute NMR | VnmrJ bug fix
| PDF, 148kB
| This document describes how to fix a bug that prevents VnmrJ on Linux from being executed as a background process.
| | Install parts list - probe and MIM | PDF, 7.9k
| Parts list for a Probe + MIM installation
| Network PING test.
| PDF, 128k
| Test your network connection to verify that the OMNMR PC and spectrometer workstation can "see" one another.
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