CapNMR Data on 1% 2-ethyl-1-indanone: 1D & 2D NMR
Important Note: These are examples from a single working system; pulse width, power level, and other parameters
Analyte: 2-ethyl-1-indanone
FW: 160.21 g/mol
Density: 1.038 g/mL
Sample: 1% 2-ethyl-1-indanone in deuterated chloroform
Total Sample Volume: 5 µL
Total Analyte Mass: 51.9 µg (0.32 µmol)
Sample Entry: Direct manual injection
For a high-mass analysis, please see our 519 µg (10%) 2-ethyl-1-indanone dataset.
Injection Method
A Hamilton Gastight 25-µL syringe was filled with clean CDCl3 solvent and used to rinse the probe. Then, 5-µL of 10% 2-ethyl-1-indanone (519 µg; 3.2 µmol; v/v in CDCl3) was drawn into the syringe and injected into the probe. Using the same syringe, 12 µL of clean CDCl3 was picked up and injected into the probe to push the 5-µL sample into the NMR flow cell of the CapNMR probe. The 12-µL Push Volume was calibrated in advance of sample injection.
Screenshots
All of the data was processed with ACD Labs SpecManager (Version. 9.0). For more information on ACD Labs and their processing and structure confirmation software, please see www.ACDLabs.com. All of the data was acquired on a Varian Inova console running Varian VnmrJ 2.1B software on a Unix workstation. A 600 MHz Oxford unshielded magnet was employed. (For more information on the Varian system, see http://www.varianinc.com/
[Click on the parameter set for a larger higher resolution image]
Proton (1H) (55 seconds)
gCOSY (Homonuclear 1H-1H) (2 minutes 53 seconds)
Tocsy (Through Multiple-Bond 1H-1H) (43 minutes 45 seconds)
gHSQC (Single Bond 1H-13C) (43 minutes 18 seconds)
Ghmbc (Multiple Bond 1H-13C) (2 hours 6 minutes)
Here is a list of Technical Bulletins that describe the setup and specific parameters for a common suite of experiments on the 5-µL of 10% 2-ethyl-1-indanone.
Tech Bulletin C0010 - Proton for CapNMR
Tech Bulletin C0020 - Direct Carbon Detection for CapNMR
Tech Bulletin C0030 - gCOSY for CapNMR
Tech Bulletin C0040 - TOCSY for CapNMR
Tech Bulletin C0050 - NOESY for CapNMR
